evangelium

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how much sodium thiosulfate should i use in description ratio ?
 

B.d.p.n.e

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evangelium

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Hi im buying all the ingredients but i cant buy 7℅ iodine tincture in my country. I can only buy tincture with sodium iodate 50℅, potassium iodide 50℅ 0.18mg/126,66℅ is it possible to use it or should i extract it somehow
 

Hypno

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Hi im buying all the ingredients but i cant buy 7℅ iodine tincture in my country. I can only buy tincture with sodium iodate 50℅, potassium iodide 50℅ 0.18mg/126,66℅ is it possible to use it or should i extract it somehow
evangeliumOrder it from aliexpres it'll be cheaper, more pure, and maybe even faster lol
 

Lordoftheshard 2

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Hi im buying all the ingredients but i cant buy 7℅ iodine tincture in my country. I can only buy tincture with sodium iodate 50℅, potassium iodide 50℅ 0.18mg/126,66℅ is it possible to use it or should i extract it somehow
evangeliumIf you need proper iodine dm me and I'll put you on tht right path fuck 7,,,, %shit hypo to if you need it
 

Hypno

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Just so eveyone knows you can buy lab grade Iodine from Aliexpress for cheap. It won't be listed as iodine but image will be iodine. I got about 100 grams a year or so ago and checked recently and there are a bunch of listings still, just gotta take your time and look, you can also find Testosterone and other things on aliexpress if you know what your doing.

Now I need to know specfics for a small red p synth. I have all the lab equipment. Don't wanna waste my PSE with a failure.
 

Lordoftheshard 2

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Just so eveyone knows you can buy lab grade Iodine from Aliexpress for cheap. It won't be listed as iodine but image will be iodine. I got about 100 grams a year or so ago and checked recently and there are a bunch of listings still, just gotta take your time and look, you can also find Testosterone and other things on aliexpress if you know what your doing.

Now I need to know specfics for a small red p synth. I have all the lab equipment. Don't wanna waste my PSE with a failure.
HypnoUse hypophosphorous acid it's cleaner lest work and you don't have to reflux for 24 hours
 

evangelium

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Hello I had a problem today with generating hydrochloride gas. I followed the video and I made the generater from gas can. I used 31% hydrochlorid acid and salt. There was no ratio of salt and hydrochloride acid so I added randomly and it didnt have the power to pushe gas through hose and it didnt bubble. I looked on internet and I found tutorial to use aluminium with hydrochloride acid. Can I use this method? The reaction was pretty short only for 5seconds. Does anyone know what was the problem with the salt and hydrochloride acid method?
 

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Hello I had a problem today with generating hydrochloride gas. I followed the video and I made the generater from gas can. I used 31% hydrochlorid acid and salt. There was no ratio of salt and hydrochloride acid so I added randomly and it didnt have the power to pushe gas through hose and it didnt bubble. I looked on internet and I found tutorial to use aluminium with hydrochloride acid. Can I use this method? The reaction was pretty short only for 5seconds. Does anyone know what was the problem with the salt and hydrochloride acid method?
evangeliumYou have to use HCl and CaCl or H2SO4 and NaCl. Use a smaller generator so you dont have to use alot of material. HCl and Al foil aren't going to do anything but make a mess.
Use a small, squeezable generator, so you can push the gas in if necessary, but make sure not to suck back your product! Try 10-15g of CaCl or NaCl and maybe 50ml or so of HCl or H2SO4. Use non iodized salt. Put everything together and block off the end of your hose and wait 5 mins for the pressure to build. Submerge your hose into your product and release the pressure, thus bubbling your gas through the product, as I said, squeeze it if necessary, but be careful.
 

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i tried to extract the rp from matches and i boiled it for 2hours with naoh solution and it turn gray it bubbled and now after washing it with distilled water it turn to grey powder and its dissapiring little bit what i did wrong ?
 

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i tried to extract the rp from matches and i boiled it for 2hours with naoh solution and it turn gray it bubbled and now after washing it with distilled water it turn to grey powder and its dissapiring little bit what i did wrong ?
evangeliumwhy would you boil the rp in naoh solution? no it shouldn't turn grey, it should still be red when you're done.
 

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evangelium
What went wrong is you boiled your RP in NaOH for 2 hours... where are you getting your instruction? I just read through this whole post and it's all here. Can you not understand the directions or are you just deciding to put your own spin on everything as you go?
 

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Like @Lordoftheshard 2 said use hypophosphoric acid for an easier and quicker method if you can find it.

Forget match strike pads if you can't get red easily, order these. https://www.aliexpress.com/w/wholes...f=auto_suggest&spm=a2g0n.productlist.header.0

Moisten slightly with acetone and let it soak a little, scrape the phosphorus off.

As for HCl generation, be careful with foil it can get violent. Keep going with non iodized salt and adding hydrochloric dropwise in a sealed vessel with a hose out the top. If you don't have lab equipment a plastic coke bottle with a small tube through the lid will do.
 
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zaners

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Like @Lordoftheshard 2 said use hypophosphoric acid for an easier and quicker method if you can find it.

Forget match strike pads if you can't get red easily, order these. https://www.aliexpress.com/w/wholes...f=auto_suggest&spm=a2g0n.productlist.header.0

Moisten slightly with acetone and let it soak a little, scrape the phosphorus off.

As for HCl generation, be careful with foil it can get violent. Keep going with non iodized salt and adding hydrochloric dropwise in a sealed vessel with a hose out the top. If you don't have lab equipment a plastic coke bottle with a small tube through the lid will do.
googieHow do you go about getting the red p off the paper? Can you just scrape it??
 
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SoldadoDeDrogas

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Is that what phosphoric acid cleaner is?
zanersThe sodium hypophosphite -> hypophosphorous acid <=> red phosphorous + I2 = Hydriodic acid. It is what Uncle Fester talks about when he goes on about the electroless nickel plating. It is sold as the 'C component'. Or 'R component' for replenisher, I believe. You may be correct I am not sure exactly how you mean. You will have to do a little research or keep asking.
 

zaners

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The sodium hypophosphite -> hypophosphorous acid <=> red phosphorous + I2 = Hydriodic acid. It is what Uncle Fester talks about when he goes on about the electroless nickel plating. It is sold as the 'C component'. Or 'R component' for replenisher, I believe. You may be correct I am not sure exactly how you mean. You will have to do a little research or keep asking.
SoldadoDeDrogasThx,I found info
 

googie

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Read through here:

 

evangelium

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How to know equal volume of water ? Do i need to calculate it threw moles ? And how can i do it ? Count it up together ? Pseudo, i2, hypo ? Is there any risks of explode or fire when do it exacly like in description ? I red that When hypophoshorus meets oxidizing agent witch is I2 or heat up more then 130° it can cought fire. Exothermic reaction is 290° so whats up with that ?
 

B.d.p.n.e

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How to know equal volume of water ? Do i need to calculate it threw moles ? And how can i do it ? Count it up together ? Pseudo, i2, hypo ? Is there any risks of explode or fire when do it exacly like in description ? I red that When hypophoshorus meets oxidizing agent witch is I2 or heat up more then 130° it can cought fire. Exothermic reaction is 290° so whats up with that ?
evangeliumI think you've put a lot of thought into the issue of equal volume, you just have to put in an equal amount or a little bit less than everything else in the balloon
 

evangelium

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I think you've put a lot of thought into the issue of equal volume, you just have to put in an equal amount or a little bit less than everything else in the balloon
B.d.p.n.eThank you for all of your advices. Im trying to uderstand it all so i wanna know all the details. So its ok to do it by eye ? I thought nothing is done by eye in chemistry
 

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Thank you for all of your advices. Im trying to uderstand it all so i wanna know all the details. So its ok to do it by eye ? I thought nothing is done by eye in chemistry
evangeliumLet me tell you the way I did itAnd I put in tap water as much as I put in for the reaction, or a little bit more than that


It's always misleading to do it by eye, but the issue of equal volume in the recipe is probably similar to this one
 

evangelium

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If it cought up how can i neutralize the fire ? Can i use normal Fire extinguisher or should i use sand ?
 

The chef

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I can get unlimited pseudoephedrine pills but I have some doubts with my pills, what happens is that they contain these active ingredients: Pseudoephedrine hydrochloride 60mg / Chlorphenamine maleate 4mg and classic excipients .....

Is there a way to extract pseudoephedrine from these pills?
( My language is Spanish but try to write in the best way. If you could help me, I would appreciate it.)
BeSZFUJwV1
 

xena

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Hey, I have a couple of questions.
1.Instead of using the ethanol/methanol mixture to separate the pills, can Dichloromethane be used instead? And will it solve the aspirin/caffeine issue?
2. What grams of iodine should be used to make the iodine solution? Or can I just shove the solid iodine straight in there? (If so what weight?) I'm using bp98
 
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