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Do you thing using 2.4 liters Phosphoric acid 85% would give out more yield?MOre
Did you basify (adding 50% Naoh) to the obtained oil after reaction?
Would you need to use vacuum for purifying that ''dirty'' oil?
Or normal steam distillation work?
I don't basify the oil layer is separated.
About purication you can choose the method that you prefer don't affect final product.