PMK Oil Synthesys From PMK (CAS 28578-16-7 Wax Form) Large Scale

[btcboss2022]

White powder starting material was this test, i also have sample from yellow waxy lumpy powder.
Swim will do a small testconversion tomorrow also on phosphoric acid...

SelassiBoth have the same behaviour but powder is more clean or pure if you prefer ;-)

 

[Selassi]

I also hear the yellow waxy one has less yield, but we will see after test

 

[Bennyboy88]

Swim already succeeded the testconversion on phosphoric acid with 500gr of 28578

SelassiThe powder u had was white or yellowish in color I notice the separation of the oil is flowing on top. Is that because u used phos acid???.

 

[btcboss2022]

Reaction scheme:
View attachment 7369

G.PattonHello,

Ratio, temperature and timing of NaHCO3 route please?
Thanks.

 

[G.Patton]

Hello,

Ratio, temperature and timing of NaHCO3 route please?
Thanks.

btcboss2022These are already written in your post, I just added scheme in order to improve and clarify information.

 

[Bennyboy88]

If phos acid will works. Woukd citrus acid can work too. Any comments anyone.

 

[G.Patton]

If phos acid will works. Woukd citrus acid can work too. Any comments anyone.

Bennyboy88Citric acid is weak, I'm not sure that it will work

 

[btcboss2022]

Hello,

Here is my last achievement make it to crystallize naturally in the molecular form of the crystal itself. More pure impossible!! ;-)
Seems handmade but trust me are naturally formed!

 

[Tweaker]

Hello,

Here is my last achievement make it to crystallize naturally in the molecular form of the crystal itself. More pure impossible!! ;-)
Seems handmade but trust me are naturally formed!

btcboss2022Very nice work. What process do you use to remove the black tar like impurity? Even on snow white crystals it appears on subsequent recrystalizations and the end product becomes quite dark.

 

[btcboss2022]

Okay thanks sounds like powder is the way to go. I have a sample amount of powder the conversion method is identical to wax?

TweakerYes exactly the same.

 

[Paranoia]

Yes exactly the same.

btcboss2022Coming next in a few weeks @btcboss2022 ice sample lab test https://analisis2.energycontrol.org/ for meth purity and eniantometer R.S

 

[Bartholomeus]

Hello,

Here is my last achievement make it to crystallize naturally in the molecular form of the crystal itself. More pure impossible!! ;-)
Seems handmade but trust me are naturally formed!

btcboss2022
What is this? Mdma Hcl ?

 

[btcboss2022]

What is this? Mdma Hcl ?

ChingShihOf course

 

[Bartholomeus]

Of course

btcboss2022
Never seen such pure mdma thats why i ask, nice

 

[btcboss2022]

Never seen such pure mdma thats why i ask, nice

ChingShihMe either until now ;-)

 

[Gale]

One of my very early synths, back when it only made sense to make product of this purity, but not very many people appreciate it for what it is..sadly.

This was back before when I did synths for a passion, being locked in labs told to make purple shit was whack.

 

[Mr Good Cat]

One of my very early synths, back when it only made sense to make product of this purity, but not very many people appreciate it for what it is..sadly.

This was back before when I did synths for a passion, being locked in labs told to make purple shit was whack.

GaleMost beautiful MDMA I've ever seen. Is it MDMA HCL? How you make it so transparent bro? I can make MDMA HCL pure white, not difficult. But still can achieve high transparency.

 

[Bennyboy88]

Well done btcboss2022. Nicest crystal I seen.

 

[Gale]

MDMA HCl -monohydrate
I moved towards making the anhydrous form, not as pretty but still similar looks

 

[Bennyboy88]

Hello,

Here is my last achievement make it to crystallize naturally in the molecular form of the crystal itself. More pure impossible!! ;-)
Seems handmade but trust me are naturally formed!

btcboss2022What method of crystallization you use to achieve these beauty. Do you mind sharing your method. Thx

 

[Gale]

I call these healing stones, for anyone wondering I used Dh20 and a gravity separation method I learned a while back inspired by JOR.

MDMA from 28578 yields a more dark brown or light yellow crystals via al/hg gassed

 

[btcboss2022]

What method of crystallization you use to achieve these beauty. Do you mind sharing your method. Thx

Bennyboy88Temp+Freeze Acetone+72hours freezer/Filter+water+temp+48 hours RT

 

[Bennyboy88]

Temp+Freeze Acetone+72hours freezer/Filter+water+temp+48 hours

btcboss2022What is the ratio of freebase:acetone. Your filtered starting powder have to be very clean in order to get clear crystal like at the end correct. Thx

 

[btcboss2022]

What is the ratio of freebase:acetone. Your filtered starting powder have to be very clean in order to get clear crystal like at the end correct. Thx

Bennyboy88Hello freebase:acetone ratio is 1:10, I dont filtered the starting powder what you mean exactly?
Thanks.